Preparation of complexes of 1-amino-6,7-O-cyclohexylidene-4-azaheptane with transition metal acetates

Oztirk O., SEKERCI M., Ozdemir E.

RUSSIAN JOURNAL OF GENERAL CHEMISTRY, cilt.76, sa.1, ss.33-36, 2006 (SCI-Expanded) identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 76 Sayı: 1
  • Basım Tarihi: 2006
  • Doi Numarası: 10.1134/s1070363206010075
  • Dergi Adı: RUSSIAN JOURNAL OF GENERAL CHEMISTRY
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Sayfa Sayıları: ss.33-36
  • Çanakkale Onsekiz Mart Üniversitesi Adresli: Evet

Özet

1-Amino-6,7-O-cyclohexylidene-4-azaheptane (L) has been synthesized starting from 1-chloro-2,3-O-cyclohexylidenepropane prepared by the reaction of epichlorohydrin with cyclohexanone, catalyzed by BF3OEt2, Complexes of this ligand with Co(II), Ni(II) and Cu(II) acetates were prepared. The structures of the ligand and its complexes are proposed based on the elemental analyses, IR, UV-VIS, and H-1 and C-13 NMR spectra, magnetic susceptibilities, and conductomety data.