CRYSTALLOGRAPHY REPORTS, cilt.58, sa.1, ss.106-110, 2013 (SCI-Expanded)
The structure of compound has also been examined cyrstallographically. It crystallizes in the monoclinic space group P2(1)/c with a = 7.673(1), b = 16.251(2), c = 10.874(1) , beta = 110.42(1)A degrees, V = 1270.7(3) (3), D (x) = 1.418 g cm(-3), R (1) = 0.0349 and wR (2) = 0.0935 [I > 2 sigma(I)], respectively. The title compound has been synthesized from the reaction of isonicotinohydrazide with 2-hydroxy-3-methoxybenzaldehyde. It has been characterized by using elemental analysis, MS, IR, H-1 NMR, C-13 NMR and UV-Visible spectroscopic techniques.