Spectroscopic studies and crystal structure of (E)-N '-(2-hydroxy-3-methoxybenzylidene)isonicotinohydrazide


Ozay H., Yildiz M., Unver H., Kiraz A.

CRYSTALLOGRAPHY REPORTS, vol.58, no.1, pp.106-110, 2013 (SCI-Expanded) identifier identifier

  • Publication Type: Article / Article
  • Volume: 58 Issue: 1
  • Publication Date: 2013
  • Doi Number: 10.1134/s1063774513010264
  • Journal Name: CRYSTALLOGRAPHY REPORTS
  • Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Page Numbers: pp.106-110
  • Çanakkale Onsekiz Mart University Affiliated: Yes

Abstract

The structure of compound has also been examined cyrstallographically. It crystallizes in the monoclinic space group P2(1)/c with a = 7.673(1), b = 16.251(2), c = 10.874(1) , beta = 110.42(1)A degrees, V = 1270.7(3) (3), D (x) = 1.418 g cm(-3), R (1) = 0.0349 and wR (2) = 0.0935 [I > 2 sigma(I)], respectively. The title compound has been synthesized from the reaction of isonicotinohydrazide with 2-hydroxy-3-methoxybenzaldehyde. It has been characterized by using elemental analysis, MS, IR, H-1 NMR, C-13 NMR and UV-Visible spectroscopic techniques.