Synthesis, Spectral Properties and Structure of New Novel 3,3'-Dibenzoyl-1,1'-(propan-1,3-diyl)-bisthiourea


AYDIN F. , Aykaç D., Unver H., Iskeleli N. O.

JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, cilt.42, ss.381-387, 2012 (SCI İndekslerine Giren Dergi) identifier identifier

  • Cilt numarası: 42 Konu: 4
  • Basım Tarihi: 2012
  • Doi Numarası: 10.1007/s10870-011-0258-5
  • Dergi Adı: JOURNAL OF CHEMICAL CRYSTALLOGRAPHY
  • Sayfa Sayıları: ss.381-387

Özet

A new 3,3'-dibenzoyl-1,1'-propan-1,3-diyl)bisthiourea was synthesized by using benzoylisothiocyanate with 1,3-diaminopropane in aprotic solvent. The structure was determinated by means of FT-IR, H-1-NMR, C-13-NMR and mass spectroscopic techniques. The crystal structure of 3,3'-dibenzoyl-1,1'-(propan-1,3-diyl)bisthiourea has also been examined by using X-ray crystallographic techniques and found to be crystallized in the monoclinic space group P2 (1) /c with the unit cell parameters: a = 5.968(1) , b = 19.471(2) , c = 16.585(2) , beta = 98.32(1)A degrees, V = 1907.0(4) (3), Dx = 1.395 g cm(-3), and Z = 4 respectively.